Mass Spectrometry in Polymer Chemistry by Christopher Barner-Kowollik, Till Gruendling, Jana

By Christopher Barner-Kowollik, Till Gruendling, Jana Falkenhagen, Steffen Weidner

Combining an up to date perception into mass-spectrometric polymer research past MALDI with program info of the instrumentation, this can be a balanced and thorough presentation of an important and normal mass-spectrometric methods.
Written through the world's so much trained specialists within the box, the ebook specializes in the most recent advancements, protecting such applied sciences and functions as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation suggestions and automatic info processing. Chapters on pattern coaching, polymer degradation and the use of mass-spectrometric instruments on an business scale around off the book.
consequently, either entrants to the sector and skilled researchers may be able to opt for the right equipment and instrumentations -- and to evaluate their respective strengths and boundaries -- for the characterization of polymer compounds.

Content:
Chapter 1 Mass research (pages 5–32): Gene Hart?Smith and Stephen J. Blanksby
Chapter 2 Ionization recommendations for Polymer Mass Spectrometry (pages 33–56): Anthony P. Gies
Chapter three Tandem Mass Spectrometry research of Polymer constructions and Architectures (pages 57–84): Vincenzo Scionti and Chrys Wesdemiotis
Chapter four Matrix?Assisted Inlet Ionization and Solvent?Free Gas?Phase Separation utilizing Ion Mobility Spectrometry for Imaging and Electron move Dissociation Mass Spectrometry of Polymers (pages 85–118): Christopher B. Lietz, Alicia L. Richards, Darrell D. Marshall, Yue Ren and Sarah Trimpin
Chapter five Polymer MALDI pattern guidance (pages 119–147): Scott D. Hanton and Kevin G. Owens
Chapter 6 floor research and Imaging recommendations (pages 149–207): Christine M. Mahoney and Dr. Steffen M. Weidner
Chapter 7 Hyphenated innovations (pages 209–235): Dr. Jana Falkenhagen and Dr. Steffen Weidner
Chapter eight computerized info Processing and Quantification in Polymer Mass Spectrometry (pages 237–280): Dr. until Gruendling, William E. Wallace, Prof. Dr. Christopher Barner?Kowollik, Charles M. Guttman and Anthony J. Kearsly
Chapter nine finished Copolymer Characterization (pages 281–318): Anna C. Crecelius and Ulrich S. Schubert
Chapter 10 Elucidation of response Mechanisms: traditional Radical Polymerization (pages 319–372): Michael Buback, Gregory T. Russell and Philipp Vana
Chapter eleven Elucidation of response Mechanisms and Polymer constitution: Living/Controlled Radical Polymerization (pages 373–403): Prof. Dr. Christopher Barner?Kowollik, Guillaume Delaittre, Dr. until Gruendling and Thomas Paulohrl
Chapter 12 Elucidation of response Mechanisms: different Polymerization Mechanisms (pages 405–436): Grazyna Adamus and Marek Kowalczuk
Chapter thirteen Polymer Degradation (pages 437–465): Paola Rizzarelli, Sabrina Carroccio and Concetto Puglisi
Chapter 14 Outlook (pages 467–468): Prof. Dr. Christopher Barner?Kowollik, Dr. Jana Falkenhagen, Dr. until Gruendling and Dr. Steffen Weidner

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Ann. Rev. Anal. , 3, 433–465. W. G. (1978) Direct analysis of mixtures by massspectrometry. Anal. , 50 (1), 81A–92A. A. G. (1978) Selected ion fragmentation with a tandem quadrupole mass-spectrometer. J. Am. Chem. , 100 (7), 2274–2275. L. E. (1984) Tandem quadrupole-time-of-flight instrument for mass-spectrometry massspectrometry. Anal. , 56 (13), 2291–2295. L. J. (2008) Hybrid mass spectrometers for tandem mass spectrometry. J. Am. Soc. , 19 (2), 161–172. A. E. (1997) Slow heating methods in tandem mass spectrometry.

Further, these classical averaging techniques are rarely capable of providing information about the various oligomers and impurities that may be present within the polymer mixture. In contrast, MS can be used for molecular mass determination, architectural elucidation, end-group analysis, quantification at trace levels, analysis of complex mixtures, and determination of degradation mechanisms [1]. Additionally, most of the classical techniques are “relative” methods that rely on calibration standards, such as polystyrene, poly (ethylene glycol), and poly(methyl methacrylate), which in many cases do not possess properties similar to the specific polymer that is being studied, and inferences must be made to yield “estimated” characterization information.

1995) Selective ionization for elemental analysis with an ion trap mass spectrometer. Spectrochimica Acta Part B, 50 (14), 1889–1895. W. (1996) Plasma source ion trap mass spectrometry: Enhanced abundance sensitivity by resonant ejection of atomic ions. J. Am. Soc. , 7 (11), 1161–1171. P. (2002) A two-dimensional quadrupole ion trap mass spectrometer. J. Am. Soc. , 13 (6), 659–669. W. (2002) A new linear ion trap mass spectrometer. Rapid Commun. , 16 (6), 512–526. M. (2005) Linear ion traps in mass spectrometry.

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